Reactivity of the biphasic trichloroacetonitrile-CH2Cl2/H2O2 system in the epoxidation of soybean oil
Annelise E. Gerbase, Márcia C. Brasil, José R. Gregório and 3 more
Grasas y Aceites · 2002
doi:10.3989/gya.2002.v53.i2.301 (opens in a new tab)
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Abstract
In this work we report on the epoxidation of soybean oil by the trichloroacetonitrile -CH2Cl2/H2O2 byphasic system. The reaction was carried out at room temperature and, most importantly, in non acid conditions which prevent the opening of the oxirane ring. The epoxidized soybean oil was characterized by infrared, 1H and 13C NMR. A maximum conversion of 81 % was achieved in two hours with 86% of selectivity in epoxy groups
Abstract licence: CC BY
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