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A facile synthesis of 3-aryl-2-mercaptoacrylic acid under microwave irradiation

Jian-Feng Zhou, Feng-Xia Zhu, Hui-Qin Zhu and 1 more

ARKIVOC · 2007

doi:10.3998/ark.5550190.0008.e20 (opens in a new tab)

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Abstract

A series of 3-aryl-2-mercaptoacrylic acid derivatives were synthesized by the hydrolysis of 5-(benzylidene)rhodanines in alkaline solution under microwave irradiation.Compared with the classical reaction conditions, this method has the advantage of excellent yields (75~94%), short reaction time (3~6 min), environmental benign, low energy consumption and easy work-up.

Abstract licence: CC BY

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