Continuous flow photolysis of aryl azides: Preparation of 3H-azepinones
Farhan R. Bou-Hamdan, François Lévesque, Alexander G. O'Brien and 1 more
Beilstein Journal of Organic Chemistry · 2011
doi:10.3762/bjoc.7.129 (opens in a new tab)
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Abstract
Photolysis of aryl azides to give nitrenes, and their subsequent rearrangement in the presence of water to give 3H-azepinones, is performed in continuous flow in a photoreactor constructed of fluorinated ethylene polymer (FEP) tubing. Fine tuning of the reaction conditions using the flow reactor allowed minimization of secondary photochemical reactions.
Abstract licence: CC BY
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