Electrogenerated base-promoted cyclopropanation using alkyl 2-chloroacetates
Kouichi Matsumoto, Yuta Hayashi, Kengo Hamasaki and 4 more
Beilstein Journal of Organic Chemistry · 2022
doi:10.3762/bjoc.18.114 (opens in a new tab)
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Abstract
The electrochemical reduction conditions of the reaction of alkyl 2-chloroacetates in Bu4NBr/DMF using a divided cell equipped with Pt electrodes to produce the corresponding cyclopropane derivatives in moderate yields were discovered. The reaction conditions were optimized, the scope and limitations, as well as scale-up reactions were investigated. The presented method for the electrochemical production of cyclopropane derivatives is an environmentally friendly and easy to perform synthetic procedure.
Abstract licence: CC BY
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