Crystal structure of hexaaquanickel(II) bis(bis(N-salicylideneglycinato- O,O′)nickelate(II)) dihydrate, [Ni(H2O)6][Ni(C9H7NO3)2] · H2O

C 36 H 44 N 4 Ni 3 O 20 , orthorhombic, Pbcn (no.60), a = 9.553(1) Å, b = 12.260(2) Å, c = 36.798(4)Å, V = 4309.8Å 3 , Z = 4, Rgt(F) = 0.059, wRref(F 2 ) = 0.144, T = 298 K. Source of materialReagents and solvents used were of commercially available quality.Salicylaldehyde (0.2 mmol, 24.5 mg) and aminoacetic acid (0.2 mmol, 15.1 mg) were dissolved in the mixture solution of methanol and water (20 ml, 2:1 v/v).The mixture was stirred for

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