Crystal structure of brevifolincarboxylic acid pyridine pentasolvate, C13H8O8 · 5 C5H5N
Lin H.-W., Xu W.-D., Wang Q.-H. and 2 more
Zeitschrift für Kristallographie - New Crystal Structures · 2005
doi:10.1524/ncrs.2005.220.4.557 (opens in a new tab)
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Abstract
C38H33N5O8, triclinic, PI (no.2), a = 11.127(2)A, b = 12.310(3) A, c = 14.266(6)A, a = 80.58(3)°, β = 69.80(3)°,γ = 73.53(2)°,V = 1753.9A 3 , Ζ = 2, R#(F) = 0.047, wR^F 2 ) = 0.157, T= 295 K. further purified by ODS column chromatography using methanol/water (2:3) as eluent to afford brevifolincarboxylic acid.The compound was crystallized from methanol to give pale yellow crystals (50 mg).Single crystals suitable for X-ray analysis were obtained by slow evaporation from pyridine at room temperature.
Abstract licence: CC BY
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