Crystal structure of methyltriphenylphosphonium bromo(pentafluorophenyl) aurate(I), [MePh3P]+[Br(C6F5)Au]-

Table 1.Parameters used for the X-ray data collectionSource of material: The title compound crystallised fortuitously from a reaction mixture in which it was a starting material.Bond lengths and angles at gold: Au-Cll 2.009(5) Â, Au-Br 2.4137(7) Â, C11 -Au-Br 177.90( 13)°.For a structure containing the related anion [CKCöFsJAu]" see réf. 1. C2sHi8AuBrF5P, monoclinic, P\2\ln\ (No. 14), a =8.875(1)Â, b =14.901(2)Â, c =18.001(2) Α, β =94.729(8)°,V =2372.5 Â 5 , Ζ =4, R(F) =0.028, tfv/F 2 ) =0.045.Crystal: colorless, equidimensional.size 0.40 χ 0.40 χ 0.40 mm Wavelength:Mo Ka radiation (0.71073 À)

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