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1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide

Hana Bashir Shawish, M. Jamil Maah, Seik Weng Ng

Acta Crystallographica Section E · 2010

doi:10.1107/s1600536810014078 (opens in a new tab)

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Abstract

In the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480 (1) Å] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O—H...O and O—H...S hydrogen bonds generate a layer motif.

Abstract licence: CC BY

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