Bis(triphenylphosphoranylidene)ammonium iodide
Michael A. Beckett, Peter N. Horton, Michael B. Hursthouse and 1 more
Acta Crystallographica Section E · 2010
doi:10.1107/s1600536810000267 (opens in a new tab)
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Abstract
The title compound, C36H30NP2+·I−, was obtained accidently from crystallization of a reaction mixture containing [(Ph3P)2N]OH and B(OH)3, which was contaminated with MeI. There are two independent [(Ph3P)2N]+ cations and two I− anions within the asymmetric unit. The central PNP angles are non-linear [137.6 (2) and 134.4 (2)°] and the phenyl substituents on P centres adopt different conformations within these two cations.
Abstract licence: CC BY
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