Chlorido(1,3-dimethylthiourea-κS)bis(triphenylphosphine-κP)copper(I) acetonitrile hemisolvate
Brian W. Skelton, Saowanit Saithong, Latipah La-o and 1 more
Acta Crystallographica Section E · 2009
doi:10.1107/s1600536809026798 (opens in a new tab)
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Abstract
The title compound, [CuCl(C3H8N2S)(C18H15P)2]·0.5CH3CN, was prepared by the reaction of copper(I) chloride with 1,3-dimethylthiourea (dmtu) and triphenylphosphine (PPh3) in acetonitrile. The CuI atom has a distorted tetrahedral environment formed by two P atoms from triphenylphosphine, one S atom from the dmtu ligand and one Cl atom. In addition, the molecules exhibit intra- and intermolecular N—H...Cl interactions.
Abstract licence: CC BY
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