Simplifying Proton NMR Spectra by Instant Homonuclear Broadband Decoupling

Abstract

Shift work: The new NMR technique, instant homonuclear decoupling, which is achieved by slice-selective homo-decoupling during acquisition, yields pure-shift NMR spectra (see picture) which can be recorded like regular 1D spectra. No special data processing is necessary and this approach can also be easily adapted for the direct dimension of two- and multidimensional spectra, giving improved resolution.

Shown for reading. Its publisher allows quoting it, not republishing it.

References 21

1. 1.

   Aguilar JA, Faulkner S, Nilsson M, Morris GA. Angew. Chem. 2010;122:3993-3995.

   Not in our library10.1002/anie.201001107

2. 2.

   Aue WP, Karhan J, Ernst RR. J. Chem. Phys. 1976;64:4226-4227.

   Not in our library

3. 3.

   Bax A, Mehlkopf AF, Smidt J. J. Magn. Reson. 1979;35:167-169.

   Not in our library

4. 4.

   Cobas JC, Martin-Pastor M. J. Magn. Reson. 2004;171:20-24.

   Not in our library10.1016/j.jmr.2004.07.016

5. 5.

   Garbow JR, Weitekamp DP, Pines A. Chem. Phys. Lett. 1982;93:504-509.

   Not in our library

6. 6.

   Luy B. J. Magn. Reson. 2009;201:18-24.

   Not in our library10.1016/j.jmr.2009.07.025

7. 7.

   Nilsson M, Morris GA. Chem. Commun. 2007;933-935.

   Not in our library10.1039/b617761a

8. 8.

   Nuzillard J. J. Magn. Reson. Ser. A. 1996;118:132-135.

   Not in our library

9. 9.

   Pell AJ, Edden RA, Keeler J. Magn. Reson. Chem. 2007;45:296-316.

   Not in our library10.1002/mrc.1966

10. 10.

    Pell AJ, Keeler J. J. Magn. Reson. 2007;189:293-299.

    Not in our library10.1016/j.jmr.2007.09.002

11. 11.

    Sakhaii P, Haase B, Bermel W. J. Magn. Reson. 2009;199:192-198.

    Not in our library10.1016/j.jmr.2009.04.016

12. 12.

    Shaka AJ, Keeler J, Freeman R. J. Magn. Reson. 1984;56:294-313.

    Not in our library

13. 13.

    Woodley M, Freeman R. J. Magn. Reson. Ser. A. 1994;111:225-228.

    Not in our library

14. 14.

    Zangger K, Sterk H. J. Magn. Reson. 1997;124:486-489.

    Not in our library

15. 15.

    Aguilar JA, Nilsson M, Morris GA. Angew. Chem. 2011;123:9890-9891.

    Not in our library10.1002/anie.201103789

16. 16.

    Lupulescu A, Olson GL, Frydman L. J. Magn. Reson. 2012;218:141-146.

    Not in our library10.1016/j.jmr.2012.02.018

17. 17.

    Kosol S, Schrank E, Bukvic-Krajacic M, Wagner GE, Meyer H, Göbl C, Zangger K, Novak P. J. Med. Chem. 2012;55:5632-5636.

    Not in our library10.1021/jm300647f

18. 18.

    Schönfeld W, Mutak S, Schönfeld W, Kirts HA. Macrolide Antibiotics. 2002;73.

    Not in our library

19. 19.

    Andreu D, Ubach J, Boman A, Wahlin B, Wade D, Merrifield RB, Boman HG. FEBS Lett. 1992;296:190-194.

    Not in our library10.1016/0014-5793(92)80377-s

20. 20.

    Respondek M, Madl T, Göbl C, Golser R, Zangger K. J. Am. Chem. Soc. 2007;129:5228-5234.

    Not in our library10.1021/ja069004f

21. 21.

    Geen H, Freeman R. J. Magn. Reson. 1991;93:93-141.

    Not in our library

Cited by papers we hold 4

• Primary Structure of Glycans by NMR Spectroscopy · 2023
  No notice
• High Resolution NMR Spectroscopy as a Structural and Analytical Tool for Unsaturated Lipids in Solution · 2017
  No notice
• Ultrahigh‐Resolution NMR Spectroscopy · 2014
  No notice
• Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy · 2013
  No notice

Reads

A person counts once a day per paper. We keep no cookie and no address: a reader is a hash that changes every day. Any month under five reads shows no number.